Chapter 1

Soil Improvement Using Grouting

A three-part investigation into cement and chemical grouting of sandy soils — from a failed laboratory carboy trial to a successful field-scale pressurized injection system, followed by chemical grouting with sodium silicate and its behavior inside concrete.

Part 1

Cement–Water Grouting

Two attempts: a laboratory trial that failed, and a field-scale pressurized system that succeeded.

Attempt 1 — LaboratoryGravity-fed, sealed carboy

Objective & Setup

Evaluate the effectiveness of cement grout in improving sandy soil inside a transparent plastic water carboy. A perforated pipe (perforations every 15 cm) delivered grout while a sealed bottom plug forced horizontal flow.

18.42 kg
Sand weight
4 : 1
W/C ratio
15 cm
Perforation spacing
Water weight
3 200 g
Cement weight
800 g
Result — Complete Failure

Grout bled to the surface and accumulated as a solid crust around the injection pipe. The soil beneath remained entirely untreated.

  • Grout failed to penetrate inter-granular voids.
  • Cement suspension separated; fluid escaped upward.
  • Rigid carboy boundary restricted natural dissipation.
  • Gravity alone could not overcome pore resistance.
Figure 1 — Failed penetration and accumulation of grout on the soil surface.
Figure 1 — Failed penetration and accumulation of grout on the soil surface.

Engineering Diagnosis

No injection pressure
Gravity flow alone could not overcome pore resistance in the sand.
Boundary & scale
Rigid plastic carboy restricted natural fluid dissipation.
High viscosity
The 4:1 mix produced particles that clogged fine sand pores.
Path of least resistance
Poor confinement allowed upward escape along the pipe.
Attempt 2 — Field Scale

Pressurized Grouting System

Modified Mix (Mix 2)

Higher fluidity via a leaner mix and a superplasticizer, injected under controlled pneumatic pressure into pre-wetted sand.

6 : 1
W/C ratio
1 %
Addicrete BVF
1 Bar
Injection pressure
Addicrete BVF — superplasticizer used to boost fluidity.
Addicrete BVF — superplasticizer used to boost fluidity.
Figure 2 — Schematic of the pressurized grouting field assembly.
Figure 2 — Schematic of the pressurized grouting field assembly.

System Components

Air compressor
Generates pneumatic pressure for injection.
Injection pipe
Delivers mix horizontally into the soil matrix.
Cement plug
Seals the upper soil collar to prevent leakage.
Grout tank
Sealed cylinder with pressure gauge.

Field Preparation

  • • Test pit excavated in natural sand to 50 cm.
  • • Surface cleared and levelled.
  • • In-situ sand containing 10% fines.

Borehole & Casing

  • • 1.0 m casing pipe, 4.5″ diameter.
  • • Perforated uniformly every 15 cm.
  • • Bottom sealed with a plug for lateral flow.

Confinement

  • • Annular cement plug, 15 cm radius, 4-day cure.
  • • Sandbag surcharge on top of cured plug.
  • • Pre-flushed with clean water before grouting.
Placing surcharge pavers around the pipe collar after the cement plug had cured.
Placing surcharge pavers around the pipe collar after the cement plug had cured.
Result — Success

Pressurized grout injection produced a consolidated, high-strength grouted soil body — confirming that pressure control, confinement, and mix fluidity are the decisive parameters.

Part 2

Chemical Grouting — Sodium Silicate (Na₂SiO₃)

A low-viscosity inorganic grout that penetrates fine voids at low pressure — with a critical limitation revealed under saturated conditions.

Key Characteristics

  • • Ultra-low viscosity (2–10 cP).
  • • High penetrability in sand & silt.
  • • Low injection pressure required.
  • • Eco-friendly, sustainable chemistry.

Reference: Warner, 2004.

Hardening Mechanism

Mixed with an activator (Calcium Chloride, CaCl₂), the reaction triggers instant polymerization, forming a dense hydrated silica gel that fills the pore spaces.

Expected Enhancements

  • • UCS: 0.5 – 3.0 MPa (sandstone-like).
  • • Permeability reduced by orders of magnitude.
  • • Effective seepage cut-off across grouted zone.
Case 1 — Dry Soil

Chemical grout successfully solidified within the sand matrix, achieving high structural cohesion and the expected strength gains.

Case 2 — Saturated Soil

Grout failed to solidify or cure — zero strength gain due to the presence of water.

Reference: Yonekura & Miwa, 1993.

Why It Fails in Saturated Ground

  • Dilution — excess pore water prevents proper polymerization.
  • Leaching — groundwater flow washes the grout away before curing.
  • Conclusion — inefficient and unsuitable for zones with high groundwater tables.
Part 3

Sodium Silicate as a Concrete Admixture

Adding Na₂SiO₃ directly to concrete mixes — a controlled destructive test on 15 × 15 × 15 cm cubes.

Mix Design (per 2 cubes)

350 kg/m³
Cement content
0.40
W/C ratio
3.071 kg
Cement
1.228 kg
Water
8.64 kg
Coarse aggregate
4.32 kg
Fine aggregate
Chemical admixture dosages
Dosage 1: 2.5% — 80 g
Dosage 2: 5.0% — 154 g

Failure Mechanisms

Flash setting
Rapid reaction with tricalcium aluminate (C₃A) traps air voids.
Disrupted hydration
Calcium silicate gel coats cement particles, blocking water.
Micro-cracking
Early shrinkage and high alkalinity induce micro-fractures.

Reference: Taylor, 1997.

28-Day Compressive Strength

MixFailure Load (kN)Compressive Strength (MPa)Change
Control (0% silicate)606.926.9100% reference
Sodium silicate 2.5%467.520.7−23.0%
Sodium silicate 5.0%380.016.8−37.5%
ADR Touch — control mix: 606.9 kN / 26.9 MPa.
ADR Touch — control mix: 606.9 kN / 26.9 MPa.
ADR Touch — 2.5% silicate: 467.5 kN / 20.7 MPa.
ADR Touch — 2.5% silicate: 467.5 kN / 20.7 MPa.
Cube crushing — 5.0% silicate: 380.0 kN / 16.8 MPa.
Cube crushing — 5.0% silicate: 380.0 kN / 16.8 MPa.
Engineering Takeaway

Inside concrete, sodium silicate acts as a structural pollutant — severely hindering standard cement hydration and producing progressively weaker mixes as dosage increases. The admixture is counterproductive for compressive strength.

Results & Discussion

Synthesis Across the Three Phases

From failed carboy trials to pressurized field grouting and the chemistry of sodium silicate.

Phase 1 — Cement Grouting Trials

Failed to achieve required permeability and homogeneous stabilization.

  • Bleeding & sedimentation: high water caused separation within 23 min.
  • Surface clogging: low water raised viscosity, blocking pores up to 60 cm.
  • Gravity limits: 1.5 m pipe height lacked pressure to overcome pore resistance.

Phase 2 — Sodium Silicate Grouting

  • • Viscosity and particle stability adjusted successfully.
  • • Full-depth penetration achieved.
  • • Homogeneous distribution throughout the sand.
  • • Increased UCS & dry density; decreased permeability.

Load–Settlement Behavior

Plate load tests compared grouted samples against a loose sand baseline (13.1 kN/m³, ultimate load 0.09 kN). Grout ratios were tested from 10:1 down to 4:1.

3-day curing
3.2× – 14×
Ultimate load vs. ungrouted sand.
7-day curing
7.7× – 14.5×
Ultimate load vs. ungrouted sand.
Load (kN)Settlement (mm)
00
0.010.03
0.020.05
0.030.07
0.040.08
0.050.13
0.070.33
0.080.44
Conclusions & Recommendations

What the Three Phases Prove

Efficiency depends strictly on grout penetration through the sand pores — controlled by viscosity, pressure, and confinement.

Viscosity link
Higher sodium silicate content increases mix viscosity, measured via Brookfield viscometer.
Two-compound system
A two-compound grout system is recommended for reliable field performance.
Bleed control
A low sodium silicate ratio prevents bleeding during injection.
Void ratio effect
Loose sand (e = 0.71): ultimate load rises 1.2–14.5×. Medium dense (e = 0.60): smaller gains.
Curing gain
Overall trend — ultimate load increases 11–21× after curing.
Permeability
Grouting significantly reduces soil permeability across the treated zone.
Settlement control
Grouting provides effective settlement control under service loads.
Foundation stabilization
Grouting reliably stabilizes foundation soils when penetration is achieved.
Continue reading
Chapter 2 — Stabilization of Silty Clay Using Cement
Go to Chapter 2
References

Chapter 1 — Bibliography

  1. 1.Clough, G. W., & Baker, W. H. (1986). Grouting for Support of Deep Excavations. Journal of Geotechnical Engineering, ASCE.
  2. 2.Hausmann, M. R. (1990). Engineering Principles of Ground Modification. McGraw-Hill.
  3. 3.Karol, R. H. (2003). Chemical Grouting and Soil Stabilization. CRC Press.
  4. 4.Mitchell, J. K., & Santamarina, J. C. (2005). Fundamentals of Soil Behavior. John Wiley & Sons.
  5. 5.Taylor, H. F. (1997). Cement Chemistry. Thomas Telford Publishing.
  6. 6.Warner, J. (2004). Practical Handbook of Grouting: Soil, Rock, and Structures. John Wiley & Sons.
  7. 7.Yonekura, R., & Miwa, M. (1993). Fundamental Properties of Sodium Silicate Grouts. Soils and Foundations.